Monday - Friday 09:00 hr to 18:00 hr
TIIR Building, NIT Campus, Rourkela, Odisha, 769008

Gas Chromatograph Mass Spectroscope

Instrument Images
CH0201

INSTRUMENT INCHARGE

Sujit Sen

Professor

Heterogeneous Catalysis: Phase Transfer Catalysis, Multiphase Reaction Engineering. Design of Experiments in Synthesis. Selectivity Engineering in Synthesis, Green Technology and Engineering. Synthesis of Zeolites and Zeolites-type material and their application. Synthesis of value-added Fine Chemicals and Petrochemicals from industrial waste materials.

BASIC INFORMATION

  • Make & Model : Agilent GC: 7980B Agilent MS: 5977A with autosampler Column available: DB5MS and DB1MS
  • Department : Chemical Engineering
  • Location : Room No. 007, Ground Floor
  • Category : Category - I
  • Status : Non-Functional

PRINCIPLE:

The GC-MS is composed of two major building blocks: the gas chromatograph and the mass spectrometer. The gas chromatograph utilizes a capillary column which depends on the columns dimensions (length, diameter, film thickness) as well as the phase properties (e.g. 5% phenyl polysiloxane). The difference in the chemical properties between different molecules in a mixture and their relative affinity for the stationary phase of the column will promote separation of the molecules as the sample travels the length of the column. The molecules are retained by the column and then elute (come off) from the column at different times (called the retention time), and this allows the mass spectrometer downstream to capture, ionize, accelerate, deflect, and detect the ionized molecules separately. The mass spectrometer does this by breaking each molecule into ionized fragments and detecting these fragments using their mass-to-charge ratio.

APPLICATION:

The GCMS system is targeted for organic, biological, pharmaceutical & polymeric sample analysis (Detection and identification). Only liquid sample with less than 1000Da.

EXPERIMENTS & CHARGES:

EXPERIMENT - 1

  • Name of Experiment : Identification of compounds
  • Condition of Analysis : AS PER MSDS DOCUMENT AND COVER LETTER
  • Service Units : 1 Sample
  • Academic & Educational Institution Charges : ₹ 1,180.00
  • R & D National Laboratory Charges : ₹ 1,180.00
  • Industry Charges : ₹ 3,540.00
  • International Charges : ₹ 11,800.00
  • Available for Sample Booking : No
  • Remarks :