National Institute of Technology Rourkela

राष्ट्रीय प्रौद्योगिकी संस्थान राउरकेला

ଜାତୀୟ ପ୍ରଯୁକ୍ତି ପ୍ରତିଷ୍ଠାନ ରାଉରକେଲା

An Institute of National Importance

Syllabus

Course Details

Subject {L-T-P / C} : CY3705 : Basic Physical Chemistry Laboratory - II { 0-0-2 / 1}

Subject Nature : Practical

Coordinator : Prof. Usharani Subuddhi

Syllabus

Accuracy, precession, errors (systematic and random), estimation of errors.
1. Determination of Order for the Persulphate-Iodide Reaction
2. Determination of the rate constant of hydrolysis of an ester in aqueous acidic medium.
3. Conductometric titration of a mixture of strong and weak acid with a strong base
4. pH metric titration of a mixture of strong and weak acid with a strong base
5. Study of the distribution equilibrium of iodine in water/tolune.
6. Adsorption charatertistics of acetic acid on charcoal
7. Verification of Beer-Lambert law.
8. Ionization constant of a weak acid (acetic acid).
9. Solubility of a sparingly soluble salt.
10. Determination of pKa values of Orhophosphoric acid using pH Meter

Course Objectives

  • These experiments are intended to acquaint the students with the practice of experimental physical chemistry.

Course Outcomes

Students are expected to understand the interconnection between experimental foundation and underlying theoretical principles and to develop laboratory skills and get familiar with a variety of physico-chemical measurement techniques.

Essential Reading

  • B. Viswanathan and P. S. Raghavan, Practical Physical Chemistry, Viva Books
  • R. C. Das and B. Behera, Experimental Physical Chemistry, Tata McGraw Hill

Supplementary Reading

  • D. Alart, Practical Physical Chemistry, Longman
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